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Expt VIIa

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Solubility Tests and Analysis
Qualitative Organic Analysis
Click below to view positive tests:

Boiling Point determination	Esters
Halogens	Phenols
Alcohols	Amines
Aldehydes	Aromatics
Ketones	Nitro-compounds

Spectroscopy Tutorial

IR Spectroscopy	http://chipo.chem.uic.edu/web1/ocol/spec/IR.htm
Mass Spectroscopy	http://chipo.chem.uic.edu/web1/ocol/spec/MS1.htm
H1 NMR Spectroscopy	http://www.cis.rit.edu/htbooks/nmr/nmr-main.htm
C13 NMR Spectroscopy	http://www.wfu.edu/~ylwong/nmr/c13/ http://edie.cprost.sfu.ca/~rhlogan/nmr.html
Chemical Shifts in C13 NMR Spectra	http://www.wfu.edu/~ylwong/nmr/c13/c13chemshift.html

Nicolet Magna-IR Spectrometer 550 A view of the sample compartment. Use the % Transmittance mode for obtaining IR sprectra.

Additional Reference Text: K.L. Williamson, Macroscale and Microscale Organic Experiments, 3rd. Edition, Houghton Mifflin Co., 1999

Expt VIIa

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